ICP atomic emission spectrometry identifies the composition and content of elements in a substance by measuring the wavelength and intensity of characteristic spectra emitted by gaseous atoms or ions of each chemical element after excitation. It is suitable for trace element analysis, applicable to most metals and a small number of non-metals such as silicon, phosphorus, and sulfur.
Instrument Model and Technical Parameters
- Instrument Model: Agilent 5110
- echnical Parameters:
- Resolution: 1 ppm
- Stability: Without internal standard correction or any form of drift correction, typical signal drift within 8 hours is < 1% RSD.
- Typical Resolution (FWHM)
元素 | 波长(nm) | 分辨率(nm) |
---|---|---|
砷 | 188.980 | <7 |
钼 | 202.032 | <7.2 |
锌 | 213.857 | <8 |
铅 | 220.353 | <8.2 |
铬 | 267.716 | <10 |
铜 | 327.396 | <13 |
钡 | 614.172 | <38 |
Sample Submission Requirements and Notes
- Sample form: Liquid or solid, weighing 100 mg–5 g.
- Solubility: Completely soluble in common inorganic solvents (e.g., water, sulfuric acid, hydrochloric acid, nitric acid, aqua regia, etc.).
Testing Examples
Implementation Standards
- ISO 19050:2021 "Raw rubber - Vulcanization characteristics - Determination of metal content by inductively coupled plasma optical emission spectrometry (ICP-OES)"
- ISO 11885:2009 "Water quality - Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES)"
- ISO 22125-2:2020 "Water quality - Determination of technetium-99 - Part 2: Inductively coupled plasma mass spectrometry (ICP-MS)"